Monday, June 29, 2009

Leather Testing Methods-Preparation of Samples for Analysis

The leather specimen for the chemical analysis is passed through a cutter mill, and the pulverized leather is called ”leather powder” or ground leather.

Suitable for this purpose are all types of mills fitted with a 4 mm screen and driven at a speed of 700 –1000 r.p.m.

Sampling according to IUC/2 and IUP/2:

1.
Sampling location for skins, whole hides and sides

Leather Sample2. Sampling location for shoulders


Leather Sample for Shoulders 3. Sampling location for bends

Leather Sample for Bends
4.
Sampling location for bellies (flanks)

Leather Sample for Bellies
a. sampling location, if no physical tests are required
b. sampling location, if physical tests are required


Regards,

Monday, June 22, 2009

Leather Testing Methods- Physical Leather Testing Method

The official methods of the International Leather Chemists’ Societies for chemical leather analysis are denoted by the letters IUC and that for the
physical testing of leather by the letters IUP. Most of them have been adopted as official methods.The letters DIN denote the official leather test methods of the German Standard Committee. Most of them have been drawn up in conformance with the IUC and IUP methods. Here we will discuss Physical Leather Testing method.


Methods of Physical Leather Testing:
IUP /1General remarks
IUP/2Sampling
= factually corresponding with DIN 53302/part 1
IUP/3Conditioning in standard atmosphere(65 ± 2 % RH and 20 ± 2 °C; DIN 50 % RH, 23 ± 2 °C)
= factually corresponding with DIN 50014-2
IUP/4Measurement of thickness
= factually corresponding with DIN 53326
IUP/5Measurement of density
= factually corresponding with DIN 53327
IUP/6 Measurement of tensile strength, elongation at break and maximumforce
= factually corresponding with DIN 53328
IUP/7Measurement of absorption of water (Kubelka)
= factually corresponding with DIN 53330
IUP/8 Measurement of tearing load
= factually corresponding with DIN 53329
IUP/9Measurement of distension and strength of grain by the ball
burst test (Lastometer)
= factually corresponding with DIN 53325
IUP/10Dynamic waterproofness test (Penetrometer)
= factually corresponding with DIN 53338/part 1
IUP/11Dynamic waterproofness test for boot and shoe sole leather
= factually corresponding with DIN 53338/part 2
IUP/12Measurement of resistance to grain cracking
= factually corresponding with DIN 53324
IUP/13Measurement of two-dimensional extension (Tensometer)
= factually corresponding with DIN 53323
IUP/14Measurement of the waterproofness of gloving leathers
= no corresponding DIN test method available
IUP/15Measurement of water vapour permeability
= factually corresponding with DIN 53333
IUP/16Measurement of shrinkage temperature
= factually corresponding with DIN 53336
IUP/17Measurement of resistance of air-dried insole leather to heat,
particularly during direct vulcanization
= no corresponding DIN test method available
IUP/18Determination of the resistance of air-dried lining leather to
heat, particularly during direct vulcanization
= no corresponding DIN test method available
IUP/19Determination of the resistance of dry upper leather to heat,
particularly in direct vulcanization and in moulding on soles
during shoe production
= no corresponding DIN test method available
IUP/20Determination of the flexing endurance of light leathers and
their surface finishes (dry and wet) in flexometer
= factually corresponding with DIN 53351
IUP/21Measurement of set in lasting with the dome plasticity apparatus
(Plastometer)
= no corresponding DIN test method available
IUP/22The assessment of surface damage by use of the viewing box
= no corresponding DIN test method available
IUP/23Measurement of damage caused by scuff
= no corresponding DIN test method available
IUP/24Measurement of surface shrinkage by immersion in hot water
IUP/26Measurement of abrasion resistance of sole leather
IUP/28Measurement of resistance to bending of heavy leather
IUP/29Determination of cold crack resistance of finishes
= factually corresponding with DIN EN ISO 13333
IUP/30Determination of water vapour absorption and desorption in
relation to dimensional changes in the leather
IUP/32Measurement of surface area (provisional draft)
= factually corresponding with ISO 11646
DIN standards not within the IUP range:
DIN 53331Determination of stitch tear strength.
DIN 53332Determination of water vapour absorption.
DIN 53340Determination of flexing endurance of low flexibility
leathers.
DIN 53344Determination of resistance for hydrolysis of finished
and unfinished leathers.
DIN 75200Determination of fire resistance.
DIN 75201Determination of fogging characteristics of trim
materials in motor vehicles.
Method A: determination with 60° reflectometer.
Method B: gravimetric determination.
DIN 75202Determination of light fastness of trim materials in
motor vehicles using the Xenon arc light.
DIN EN 344-1Protective shoes.
DIN EN 374-1Protective gloves.

DIN EN ISO 105B-02 Colour fastness to artificial light.

Regards,

Leather Testing Methods by Padana

PADANA GARMENTS is one of the few companies in the world with full wet-end development and production capabilities. From preserving hides, to following precise steps in the manufacturing process, we exercise the complete control that ensures our leather is the most acclaimed in the industry.
Leather Testing Methods:

Here are some of the details of Leather Testing Methods;

IUC/IUP-methodsThe official methods of the International Leather Chemists’ Societies for chemical leather analysis are denoted by the letters IUC and that for the physical testing of leather by the letters IUP. Most of them have been adopted as official methods. The letters DIN denote the official leather test methods of the German Standard Committee. Most of them have been drawn up in conformance with the IUC and IUP methods.

Methods of chemical leather analysis:

IUC/1General remarks and presentation of analytical results
= factually corresponding with DIN 53300/part 2
IUC/2Sampling (as in IUP/2)
= factually corresponding with DIN 53302/part 2
IUC/3Preparing the test material by disintegration
= factually corresponding with DIN EN ISO 4044
IUC/4Determination of substances extractable with dichloromethane
= factually corresponding with DIN EN ISO 4048
IUC/5Determination of the water content of leather
= factually corresponding with DIN 53304
IUC/6Determination of organic and inorganic substances in leather removable by washing (loss by washing)
= factually corresponding with DIN 53307
IUC/7Determination of ash and water-insoluble mineral substances
= factually corresponding with DIN EN ISO 4047
IUC/8Determination of chromium content
= factually corresponding with DIN 53309
IUC/9Determination of water soluble magnesium salts in leather (epsom salt)
= factually corresponding with DIN EN ISO 5399
IUC/10Determination of nitrogen, ammonium and skin substance
= factually corresponding with DIN 53308
IUC/11Determination of pH and difference value of aqueous leather extract
= factually corresponding with DIN EN ISO4045
IUC/13Determination of zirconium
= no corresponding DIN test method available
IUC/15Determination of phosphorus
= no corresponding DIN test method available
IUC/16Determination of aluminium
= no corresponding DIN test method available
IUC/17Determination of hydroxyproline
= no corresponding DIN test method available

DIN standards not within the IUC range


DIN 53314 Determination of chromium (VI) compounds in leather
DIN 53315 Determination of formaldehyde in leather

The following methods are in the course of preparation and have not yetbeen adopted as official methods:
a. Determination of iron in leather
b.
Determination of free fatty acids in leather
c. Determination of extractable fat (chamois leather)
d.
Determination of sulfur in leather
e. Determination of glutaraldehyde in leather
f.
Determination of pentachlorophenol (PCP) in leather

Rgards,